Fast Screening of Firearm Discharge Residues by Laser-based Spectrochemical Methods, Electrochemical Sensors, and Chemometrics, West Virginia, 2019-2021 (ICPSR 38296)

Version Date: Apr 16, 2026 View help for published

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Tatiana Trejos, West Virginia University

https://doi.org/10.3886/ICPSR38296.v1

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The detection of gunshot residue (GSR) provides valuable information in violent crimes, accidental shootings, and terrorism. Despite the scientific validity of this discipline, there are persistent challenges regarding the speed of analysis, preservation of the evidence, and interpretation of results. Consequently, there is a critical need to improve the discipline's turnaround times and reliability. This study's overall purpose was to develop a comprehensive approach to overcome these significant concerns and enhance the criminal justice system capabilities. This project developed and validated fast and reliable tests, using laser-induced breakdown spectroscopy (LIBS) and electrochemical (EC) sensors for GSR detection. Also, statistical models were applied for the quantitative interpretation of the evidence. The combination of LIBS and EC data permitted the accurate identification of organic and inorganic residues (OGSR and IGSR, accuracy ranging from 92-99% depending on the subpopulation and classification models). This research focused on developing SMARTER (Simpler, Modern, Affordable, Rapid, Transformative, Effective, and Reliable) solutions for GSR examinations.

The main objectives were:

  1. Application of universal and expanded collection methods
  2. Development of novel, ultrafast methods for dual detection of IGSR and OGSR
  3. Development of modern 3D chemical imaging for crime scene reconstruction
  4. Development of novel micro-particle GSR standards
  5. Creation of a large population study and probabilistic interpretation framework

Trejos, Tatiana. Fast Screening of Firearm Discharge Residues by Laser-based Spectrochemical Methods, Electrochemical Sensors, and Chemometrics, West Virginia, 2019-2021. Inter-university Consortium for Political and Social Research [distributor], 2026-04-16. https://doi.org/10.3886/ICPSR38296.v1

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United States Department of Justice. Office of Justice Programs. National Institute of Justice (2018-DU-BX-0186)
Inter-university Consortium for Political and Social Research
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2019 -- 2021
2019-06 -- 2021-03
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For this large population study to observe the trends in both the background population and known shooter, a total of 1,061 sets were collected. All participants were asked to volunteer for the study and were not required to participate. 455 of those sets were collected from the background population (350 low-risk and 105 high-risk) from individuals who had not fired a weapon with 24 hours of collection. The high-risk sets were collected from individuals who had hobbies and professions with a potential for more false positives (mechanics, agriculture workers, firearm researchers, and police officers and their administrators). A total of 606 known shooter sets were collected using different types of ammunition and originated from four main sub-populations: 200 leaded shooter sets, 86 activity sets, 100 lead-free sets, and 220 mixed leaded and lead-free sets.

The data collected was from over 1,000 participants resulting in over 3,200 individual samples and generating over 100,000 data sets.

Cross-sectional

Volunteers from the background population and known shooter samples.

Other
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2026-04-16

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Notes

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